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发 送 文 章     C.I. 酸性蓝129 (C.I. 62508) 生产工艺 [留言][评论][收藏] 收信地址     填写收信人的电子邮箱 邮件主题     填写邮件主题 邮件内容  <p class="MsoNormal"> <span><span>              </span><strong><u>C.I. </u></strong></span><strong><u><span style="font-family:宋体;">酸性蓝</span><span>129 (C.I. 62508) </span></u></strong><strong><u><span style="font-family:宋体;">生产工艺</span> </u><span><span>             </span>CAS</span></strong><strong><span style="font-family:宋体;">号：</span><span>[6397-02-0]</span></strong> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;">CAS</span></u></strong><strong><u><span style="font-size:9.0pt;font-family:宋体;">名：</span></u></strong><strong><span style="font-size:9.0pt;"> 2-Anthracenesulfonc acid, </span></strong><span style="font-size:9.0pt;">1-amino-9,10-dihydro-9,10dioxo-4-[(2,4,6-trimethylphenyl)amino]- </span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span>                                 </span>monosodium salt. </span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">用途：</span></u></strong><span style="font-size:9.0pt;"> 1. </span><span style="font-size:9.0pt;font-family:宋体;">染色用。</span><span style="font-size:9.0pt;"><span>  </span>2. </span><span style="font-size:9.0pt;font-family:宋体;">合成酸性紫</span><span style="font-size:9.0pt;">48</span><span style="font-size:9.0pt;font-family:宋体;">；</span><span style="font-size:9.0pt;">126</span><span style="font-size:9.0pt;font-family:宋体;">。酸性蓝</span><span style="font-size:9.0pt;">260. </span><span style="font-size:9.0pt;font-family:宋体;">溶剂蓝</span><span style="font-size:9.0pt;">136.</span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">合成路线：</span></u></strong><strong><u><span style="font-size:9.0pt;"></span></u></strong> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><img alt="" title="" src="http://www.陈忠源化学文库.cn//chenzhongyuan/Upload/ArticlePicture/1.png" align="" width="481" height="154" /></span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">生产工艺：</span></u></strong><span style="font-size:9.0pt;"><span>  </span></span><span style="font-size:9.0pt;font-family:宋体;">英文抄录如下：</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span>    </span>1-Amino-4-bromo-anthraquinone-2-sulfonic acid (40 kg. 100%) as sodium salt is stirred into water 250 litre, ethanol 100 litre, mesidine 916 litre, sodium hydrogencarbonate 30 kg. and glucose 6 kg. are then added to the suspension, which is stirred and heated to 40<sup>0</sup>C., cuprous chloride 1 kg. is added and the temperature raised to 70<sup>0</sup>C. and maintained at 70-75<sup>0</sup>C. for 2 hours. On cooling to 55<sup>0</sup>C., the precipitated dye is filtered, wahed with sodium hydrogencarbonate solution (400 litre, 5%) at 50<sup>0</sup>C., and then dried at 80<sup>0</sup>C. to give a yield of 40 kg. The product dyes wool and nylon in bright reddish-blue hues of good light and wet fastness.</span> <br /> <p class="MsoNormal" style="text-indent:17.25pt;"> <span style="font-size:9.0pt;font-family:宋体;">抄自：</span><span style="font-size:9.0pt;">Handbook of Export oriented Dyes and Intermediates Industry. 1994. P. 437. </span><span style="font-size:9.0pt;font-family:宋体;">印度。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">实验室合成方法：</span></u></strong><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal" style="text-indent:17.25pt;"> <span style="font-size:9.0pt;font-family:宋体;">上海染化六厂</span><span style="font-size:9.0pt;"> -1979</span><span style="font-size:9.0pt;font-family:宋体;">年</span><span style="font-size:9.0pt;">8</span><span style="font-size:9.0pt;font-family:宋体;">月。略。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">参考文献：</span></u></strong><strong><u><span style="font-size:9.0pt;"></span></u></strong> <br /> <p class="MsoNormal" style="text-indent:17.25pt;"> <span style="font-size:9.0pt;font-family:宋体;">染料工业，染料与染色。</span><span style="font-size:9.0pt;"><span>  </span>1979, 6, 39-42; 1984, 3, 5-6; 2001, 3,9; 2009, 46(5), 25-7</span> <br /> <p class="MsoNormal" style="text-indent:17.25pt;"> <span style="font-size:9.0pt;font-family:宋体;">上海染料。</span><span style="font-size:9.0pt;"> 1999, 6, 18-21.</span> <br /> <p class="MsoNormal" style="text-indent:17.25pt;"> <span style="font-size:9.0pt;font-family:宋体;">日本化药染料便览。</span><span style="font-size:9.0pt;"> <span>P. 332-3 </span></span><span style="font-size:9.0pt;font-family:宋体;">染色数据。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">不同成盐体：</span></u></strong><strong><u><span style="font-size:9.0pt;"></span></u></strong> <br /> <p class="MsoNormal"> <u><span style="font-size:9.0pt;"><span>  </span></span></u><u><span style="font-size:9.0pt;font-family:宋体;">分子式</span></u><u><span style="font-size:9.0pt;"><span>            </span>CAS</span></u><u><span style="font-size:9.0pt;font-family:宋体;">号</span></u><u><span style="font-size:9.0pt;"><span>       </span>EC</span></u><u><span style="font-size:9.0pt;font-family:宋体;">号</span></u><u><span style="font-size:9.0pt;"><span>              </span></span></u><u><span style="font-size:9.0pt;font-family:宋体;">备注</span></u><u><span style="font-size:9.0pt;"><span>     </span><span>                                   </span></span></u> <br /> <p class="MsoNormal"> <strong><span style="font-size:9.0pt;">C<sub>23</sub>H<sub>20</sub>N<sub>2</sub>O<sub>5</sub>S</span></strong><span style="font-size:9.0pt;"><span>          </span>1833-57-4<span>   </span>217-394-7</span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;">------“--------. Na<span>       </span>6397-02-0<span>   </span>229-008-4<span>      </span></span><span style="font-size:9.0pt;font-family:宋体;">酸性蓝</span><span style="font-size:9.0pt;">129</span><span style="font-size:9.0pt;font-family:宋体;">，钠盐。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;">------“--------. Li<span>       </span>72927-96-9<span>   </span>277-037-6<span>      </span></span><span style="font-size:9.0pt;font-family:宋体;">酸性蓝</span><span style="font-size:9.0pt;">129</span><span style="font-size:9.0pt;font-family:宋体;">，锂盐。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;">------“--------.<span>          </span>----</span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span> </span>.C<sub>12 – 14</sub> tett alkylammium<span>          </span>414-110-5<span>      </span></span><span style="font-size:9.0pt;font-family:宋体;">溶剂蓝</span><span style="font-size:9.0pt;">136.<span>  </span>EP. 445075. 1991</span><span style="font-size:9.0pt;font-family:宋体;">年。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;">------“--------.Na</span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span> </span>Comp. with<span>        </span>52619-53-1<span>     </span>---<span>           </span>N,N-dibutyl-1-butanamine</span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;">------“--------.</span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"> </span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"> </span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"> </span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"> </span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"> </span> <br /> <p class="MsoNormal"> <strong><span style="font-size:9.0pt;font-family:宋体;">陈忠源</span></strong><strong><span style="font-size:9.0pt;"><span>  </span>2016</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">年</span></strong><strong><span style="font-size:9.0pt;">2</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">月</span></strong><strong><span style="font-size:9.0pt;">29</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">日。</span></strong><strong><span style="font-size:9.0pt;"></span></strong> <br /><br /><br />本文地址：<a href="http://www.陈忠源化学文库.cn/Article.asp?ID=10000061" target="_blank">http://www.陈忠源化学文库.cn/Article.asp?ID=10000061</a>   填写邮件内容   邮件签名     填写邮件签名 发信地址     填写发信人的电子邮箱 　验证码     填写验证码，单击即可刷新验证码   发送协议 ·欢迎使用本站在线文章发送系统。 ·不得使用本站在线发送邮件系统发送垃圾邮件、广告邮件。 ·如果收信人地址或其服务器出现错误，可能无法成功发送。 ·如果有什么问题，或者意见建议，请联系[网站管理员]。

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