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发 送 文 章     C.I. 酸性绿25 = C.I.酸性绿95 (C.I. 61570) 生产工艺 [留言][评论][收藏] 收信地址     填写收信人的电子邮箱 邮件主题     填写邮件主题 邮件内容  <p class="MsoNormal"> <strong><span><span><u>C.I. </u></span></span></strong><span><span><strong><u><span style="font-family:宋体;">酸性绿</span><span>25 = C.I.</span></u></strong></span></span><span><span><strong><u><span style="font-family:宋体;">酸性绿</span><span>95 (C.I. 61570) </span></u></strong></span></span><span><span><strong><u><span style="font-family:宋体;">生产工艺</span></u></strong></span></span><strong><u> </u><span><span>       </span>CAS</span></strong><strong><span style="font-family:宋体;">号</span><span>: [4403-90-1]</span></strong> <p class="MsoNormal"> <strong><span><u>C.I. </u></span></strong><strong><u><span style="font-family:宋体;">溶剂绿</span><span> 3 = C.I. </span></u></strong><strong><u><span style="font-family:宋体;">分散绿</span><span>6:1 (C.I. 61565) </span></u></strong><strong><u><span style="font-family:宋体;">生产工艺</span> </u><span><span>        </span>CAS</span></strong><strong><span style="font-family:宋体;">号</span><span>:[128-80-3]</span></strong> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;">CAS</span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">名：</span></u></strong><strong><span style="font-size:9pt;"> Benzenesulfonic acid, </span></strong><span style="font-size:9pt;">2,2’-[(9,10-dihydro-9,10-dioxo-1,4-anthracenediyl)diimino]bis[5-methyl]-</span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;"><span>        </span>Disodium salt.<span>  </span>= C.I. </span><span style="font-size:9pt;font-family:宋体;">酸性绿</span><span style="font-size:9pt;">25.</span> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;">CAS</span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">名：</span></u></strong><strong><span style="font-size:9pt;"> 9,10-Anthracenedione,</span></strong><span style="font-size:9pt;"> 1,4-bis[(4-methylphenyl)amino]-<span>   </span>= C.I. </span><span style="font-size:9pt;font-family:宋体;">溶剂绿</span><span style="font-size:9pt;">3.</span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;font-family:宋体;">发明者：</span></u></strong><span style="font-size:9pt;"><span>  </span>R. E. Schmidt 1894</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;font-family:宋体;">生产工艺文献：</span></u></strong><strong><span style="font-size:9pt;"><span>  </span>FIAT 1313,</span></strong><span style="font-size:9pt;"> II, 215.<span>   </span></span><span style="font-size:9pt;font-family:宋体;">德文摘要的英文摘译文。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;">  <strong>FIAT 764 – Alizarincyaningruen G.<span>  </span></strong>“Color Index” </span><span style="font-size:9pt;font-family:宋体;">未说明</span><span style="font-size:9pt;">PB</span><span style="font-size:9pt;font-family:宋体;">报告号。</span><span style="font-size:9pt;"></span> <br />   <strong><span style="font-size:9pt;">PB 82232, </span></strong><span style="font-size:9pt;">856-857. <strong>Alizarincyaningruen G </strong>extra. <strong><span> </span></strong></span><span style="font-size:9pt;font-family:宋体;">应调査团要求编写的德文简要生产工艺。</span><span style="font-size:9pt;"> 2</span><span style="font-size:9pt;font-family:宋体;">美元。</span><span style="font-size:9pt;"></span> <br />   <strong><span style="font-size:9pt;">PB 82232, </span></strong><span style="font-size:9pt;">1009-1010. <strong>Alizarincyaningruen </strong>fat soluble = C.I. </span><span style="font-size:9pt;font-family:宋体;">溶剂绿</span><span style="font-size:9pt;">3.<span>  </span></span><span style="font-size:9pt;font-family:宋体;">同上。</span><span style="font-size:9pt;"> 2</span><span style="font-size:9pt;font-family:宋体;">美元。</span><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">未抄录。<br />   </span><u><span style="font-size:9pt;font-family:宋体;">茜素化青绿</span></u><u><span style="font-size:9pt;">G extra</span></u><u><span style="font-size:9pt;font-family:宋体;">生产工艺</span></u><u><span style="font-size:9pt;"> </span></u> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;font-family:宋体;">反应式：</span></u></strong><span style="font-size:9pt;"><span>  </span></span><span style="font-size:9pt;font-family:宋体;">为本人加注，原件未列。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;"><img alt="" src="data:image/png;base64,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" /></span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;"><img alt="" src="data:image/png;base64,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" /></span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;">1.<span>  </span></span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">色基生产：</span></u></strong><span style="font-size:9pt;"><span>  </span>C.I. </span><span style="font-size:9pt;font-family:宋体;">溶剂绿</span><span style="font-size:9pt;">3.= C.I. </span><span style="font-size:9pt;font-family:宋体;">分散绿</span><span style="font-size:9pt;">6:1.</span> <br /> <p class="MsoNormal"> <u><span style="font-size:9pt;font-family:宋体;">设备：</span></u><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">略！</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <u><span style="font-size:9pt;font-family:宋体;">操作步骤：</span></u><u><span style="font-size:9pt;"></span></u> <br />   <span style="font-size:9pt;font-family:宋体;">在</span><span style="font-size:9pt;">1000</span><span style="font-size:9pt;font-family:宋体;">升搪瓷锅内，加入</span><span style="font-size:9pt;">750</span><span style="font-size:9pt;font-family:宋体;">公斤熔融的对甲苯胺，</span><span style="font-size:9pt;">150</span><span style="font-size:9pt;font-family:宋体;">公斤工业</span><span style="font-size:9pt;">1,4-</span><span style="font-size:9pt;font-family:宋体;">二羟基蒽醌，</span><span style="font-size:9pt;">60</span><span style="font-size:9pt;font-family:宋体;">升工业盐酸和</span><span style="font-size:9pt;">15</span><span style="font-size:9pt;font-family:宋体;">公斤硼酸，加热到</span><span style="font-size:9pt;">85<sup>0</sup>C.</span><span style="font-size:9pt;font-family:宋体;">，在</span><span style="font-size:9pt;">85<sup>0</sup>C.</span><span style="font-size:9pt;font-family:宋体;">加入锌粉，加料过程温度能自行升高到</span><span style="font-size:9pt;">92<sup>0</sup>C.,</span><span style="font-size:9pt;font-family:宋体;">加毕在</span><span style="font-size:9pt;">92<sup>0</sup>C.</span><span style="font-size:9pt;font-family:宋体;">反应到取样不再有反应为止，一般需</span><span style="font-size:9pt;">3-4</span><span style="font-size:9pt;font-family:宋体;">小时。合格后冷却至</span><span style="font-size:9pt;">70<sup>0</sup>C.</span><span style="font-size:9pt;font-family:宋体;">，放料到已加有</span><span style="font-size:9pt;">750</span><span style="font-size:9pt;font-family:宋体;">升甲醇的</span><span style="font-size:9pt;">2500</span><span style="font-size:9pt;font-family:宋体;">升稀释锅内，冷至</span><span style="font-size:9pt;">20<sup>0</sup>C.</span><span style="font-size:9pt;font-family:宋体;">，压滤，滤饼用甲醇洗涤四次，每次</span><span style="font-size:9pt;">200</span><span style="font-size:9pt;font-family:宋体;">升，母液和洗液收集到</span><span style="font-size:9pt;">4000</span><span style="font-size:9pt;font-family:宋体;">升受槽内。滤饼再用清水洗五次，每次</span><span style="font-size:9pt;">200</span><span style="font-size:9pt;font-family:宋体;">升，洗水收集到洗水受槽内。</span><span style="font-size:9pt;"></span> <br /> <span style="font-size:9pt;font-family:宋体;"><span style="font-family:Tahoma;">  </span>甲醇对甲苯胺液，用水蒸汽蒸馏回收，对甲苯胺用耙式干燥器，蒸馏回收。</span><span style="font-size:9pt;"></span> <br />   <strong><span style="font-size:9pt;font-family:宋体;">得量</span></strong><strong><span style="font-size:9pt;">: <span> </span></span></strong><span style="font-size:9pt;">416</span><span style="font-size:9pt;font-family:宋体;">公斤湿品，含量：</span><span style="font-size:9pt;">50%</span><span style="font-size:9pt;font-family:宋体;">。</span><span style="font-size:9pt;"></span> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;">2.<span>  </span></span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">染料生产：</span></u></strong><span style="font-size:9pt;"><span>  </span>C.I. </span><span style="font-size:9pt;font-family:宋体;">酸性绿</span><span style="font-size:9pt;">25.= C.I. </span><span style="font-size:9pt;font-family:宋体;">酸性绿</span><span style="font-size:9pt;">95.</span> <br /> <p class="MsoNormal"> <u><span style="font-size:9pt;font-family:宋体;">操作步骤：</span></u><u><span style="font-size:9pt;"></span></u> <br />   <span style="font-size:9pt;font-family:宋体;">在</span><span style="font-size:9pt;">1000</span><span style="font-size:9pt;font-family:宋体;">升磺化锅内，加入预先由</span><span style="font-size:9pt;">310</span><span style="font-size:9pt;font-family:宋体;">升</span><span style="font-size:9pt;">20%</span><span style="font-size:9pt;font-family:宋体;">发烟硫酸和</span><span style="font-size:9pt;">110</span><span style="font-size:9pt;font-family:宋体;">升</span><span style="font-size:9pt;">96%</span><span style="font-size:9pt;font-family:宋体;">硫酸配成的</span><span style="font-size:9pt;">8-10%</span><span style="font-size:9pt;font-family:宋体;">发烟硫酸，然后冷却至</span><span style="font-size:9pt;">30<sup>0</sup>C.</span><span style="font-size:9pt;font-family:宋体;">以下，通过筛网加入</span><span style="font-size:9pt;">200</span><span style="font-size:9pt;font-family:宋体;">公斤色基，加毕追加</span><span style="font-size:9pt;">150</span><span style="font-size:9pt;font-family:宋体;">升</span><span style="font-size:9pt;">20%</span><span style="font-size:9pt;font-family:宋体;">发烟硫酸，磺化到取样溶于水为止。</span><span style="font-size:9pt;"></span> <br />   <span style="font-size:9pt;font-family:宋体;">稀释锅内先加水</span><span style="font-size:9pt;">4500</span><span style="font-size:9pt;font-family:宋体;">升，加入</span><span style="font-size:9pt;">375</span><span style="font-size:9pt;font-family:宋体;">公斤食盐和</span><span style="font-size:9pt;">2</span><span style="font-size:9pt;font-family:宋体;">升亚硫酸氢钠溶液，然后接受磺化料，稀释后压滤，滤饼用由</span><span style="font-size:9pt;">4500</span><span style="font-size:9pt;font-family:宋体;">升水和</span><span style="font-size:9pt;">300</span><span style="font-size:9pt;font-family:宋体;">公斤食盐配成的盐水洗涤。</span><span style="font-size:9pt;"></span> <br />   <span style="font-size:9pt;font-family:宋体;">滤饼用</span><span style="font-size:9pt;">200-300</span><span style="font-size:9pt;font-family:宋体;">水打浆，加入</span><span style="font-size:9pt;">50-200</span><span style="font-size:9pt;font-family:宋体;">公斤</span><span style="font-size:9pt;">30%</span><span style="font-size:9pt;font-family:宋体;">氢氧化钠液中和后，于减压干燥器内干燥。</span><span style="font-size:9pt;"></span> <br />   <strong><span style="font-size:9pt;font-family:宋体;">得量：</span></strong><strong><span style="font-size:9pt;"> 388.5</span></strong><span style="font-size:9pt;font-family:宋体;">公斤，</span><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">合标准染料</span><span style="font-size:9pt;"> = 518</span><span style="font-size:9pt;font-family:宋体;">公斤茜素化青绿</span><span style="font-size:9pt;">G extra.</span> <p class="MsoNormal"> <strong><span style="font-size:9pt;font-family:宋体;">陈忠源</span></strong><strong><span style="font-size:9pt;"><span>    </span></span></strong><span style="font-size:9pt;">1980</span><span style="font-size:9pt;font-family:宋体;">年</span><span style="font-size:9pt;">11</span><span style="font-size:9pt;font-family:宋体;">月</span><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">译自</span><strong><span style="font-size:9pt;">PB</span></strong><span style="font-size:9pt;"> 82232, 856-7. (</span><span style="font-size:9pt;font-family:宋体;">德文</span><span style="font-size:9pt;">)</span><span style="font-size:9pt;font-family:宋体;">。</span><span style="font-size:9pt;">FIAT 1313,II, 215. </span><span style="font-size:9pt;font-family:宋体;">是它的英文译文。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;font-family:宋体;">合成工艺参考文献：</span></u></strong><strong><u><span style="font-size:9pt;"></span></u></strong> <br /> <p class="MsoNormal"> <span style="font-size:9pt;">1. </span><span style="font-size:9pt;font-family:宋体;">酸性媒介绿</span><span style="font-size:9pt;">GS</span><span style="font-size:9pt;font-family:宋体;">中试操作法。</span><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">染料工业</span><span style="font-size:9pt;"> 1975, 1. 56; 1976, 1,68.</span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;">2. </span><span style="font-size:9pt;font-family:宋体;">酸性绿</span><span style="font-size:9pt;">GS</span><span style="font-size:9pt;font-family:宋体;">扩大试验报告。</span><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">染料工业</span><span style="font-size:9pt;"> 1975, 3, 55.</span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;">3. </span><span style="font-size:9pt;font-family:宋体;">酸性蒽醌绿生产工艺</span><span style="font-size:9pt;"><span>  </span></span><span style="font-size:9pt;font-family:宋体;">译自俄，有机染料及中间体生产工艺学。</span><span style="font-size:9pt;">P. 369-372.<span>  </span>1980</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;">4. </span><span style="font-size:9pt;font-family:宋体;">油溶性蒽醌绿</span><span style="font-size:9pt;"><span>  </span></span><span style="font-size:9pt;font-family:宋体;">译自俄，染料及中间体实验室合成方法。§</span><span style="font-size:9pt;">5.17.<span>  </span>1985</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;">5. </span><span style="font-size:9pt;font-family:宋体;">酸性蒽醌绿</span><span style="font-size:9pt;"><span>    </span></span><span style="font-size:9pt;font-family:宋体;">译自俄，染料及中间体实验室合成方法。§</span><span style="font-size:9pt;">5.18.<span>  </span>1985</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;"> </span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;font-family:宋体;">关于溶剂绿</span></u></strong><strong><u><span style="font-size:9pt;">3 = </span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">分散绿</span></u></strong><strong><u><span style="font-size:9pt;">6:1</span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">：</span></u></strong><strong><u><span style="font-size:9pt;"></span></u></strong> <br /> <p class="MsoNormal"> <span style="font-size:9pt;font-family:宋体;">非纺织品用：</span><span style="font-size:9pt;">1. Kosmetische Faerbemittel / Colour for Cosmetics.<span>  </span>C-Gruen 10 (3</span><span style="font-size:9pt;font-family:宋体;">页</span><span style="font-size:9pt;">)<span>  </span>1984</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;"><span>      </span>2. Coloring of Foods,Drugs and Cosmetics.<span>  </span>P. 257-8.<span>   </span>1999</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <p class="MsoNormal"> <span style="font-size:9pt;font-family:宋体;">复配：</span><span style="font-size:9pt;">EC 905-528-3 </span><span style="font-size:9pt;font-family:宋体;">和</span><span style="font-size:9pt;"> EC 905-529-9.</span> <p class="MsoNormal"> <strong><u><span style="font-size:9pt;font-family:宋体;">关于酸性绿</span></u></strong><strong><u><span style="font-size:9pt;">25</span></u></strong><strong><u><span style="font-size:9pt;font-family:宋体;">：</span></u></strong><strong><u><span style="font-size:9pt;"></span></u></strong> <br /> <p class="MsoNormal"> <span style="font-size:9pt;font-family:宋体;">染色性能：</span><span style="font-size:9pt;font-family:宋体;">见“日本化药染料便览”</span><span style="font-size:9pt;"> p. 340-341. 1982</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <p class="MsoNormal"> <span style="font-size:9pt;font-family:宋体;">非纺织品用：</span><span style="font-size:9pt;"> </span><span style="font-size:9pt;font-family:宋体;">同上。</span><span style="font-size:9pt;"> 1. <span> </span>C-Gruen 11 (3</span><span style="font-size:9pt;font-family:宋体;">页</span><span style="font-size:9pt;">) 1984</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"><span>  </span>2. <span> </span>P. 259-60.<span>  </span>1999</span><span style="font-size:9pt;font-family:宋体;">年。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9pt;font-family:宋体;">不同成盐体：如下。</span><span style="font-size:9pt;"></span> <br /> <p class="MsoNormal"> <u><span style="font-size:9pt;"><span>  </span></span></u><u><span style="font-size:9pt;font-family:宋体;">分子式</span></u><u><span style="font-size:9pt;"><span>   </span><span>    </span>CAS</span></u><u><span style="font-size:9pt;font-family:宋体;">号</span></u><u><span style="font-size:9pt;"><span>    </span>EC</span></u><u><span style="font-size:9pt;font-family:宋体;">号</span></u><u><span style="font-size:9pt;"><span>     </span></span></u><u><span style="font-size:9pt;font-family:宋体;">备注</span></u> <p class="MsoNormal"> <strong><span style="font-size:9pt;">C<sub>28</sub>H<sub>22</sub>N<sub>2</sub>O<sub>8</sub>S<sub>2</sub><span>     </span></span></strong><span style="font-size:9pt;">3443-90-1 </span> <p class="MsoNormal"> <span style="font-size:9pt;">-----“----------.     94020-96-9<span>   </span>301-391-3    </span><span style="font-size:9pt;font-family:宋体;">磺酸基不定位。</span><span style="font-size:9pt;"></span> <p class="MsoNormal"> <span style="font-size:9pt;">-----“----------.2 Na    4403-90-1<span>   </span>224-546-6</span> <p class="MsoNormal"> <span style="font-size:9pt;">-----“----------.x Na<span>    </span>68039-54-3<span>   </span>268-267-8</span> <p class="MsoNormal"> <span style="font-size:9pt;">-----“----------.x Na<span>    </span>85248-90-4<span>   </span>286-463-1</span> <p class="MsoNormal"> <span style="font-size:9pt;">-----“----------. 2 K    83044-88-6<span>   </span>280-170-2    </span><span style="font-size:9pt;font-family:宋体;">甲基，磺酸基不定位。</span><span style="font-size:9pt;"></span> <p class="MsoNormal"> <strong><span style="font-size:9pt;font-family:宋体;">陈忠源</span></strong><strong><span style="font-size:9pt;"><span>  </span></span></strong><span style="font-size:9pt;">2016</span><span style="font-size:9pt;font-family:宋体;">年</span><span style="font-size:9pt;">3</span><span style="font-size:9pt;font-family:宋体;">月</span><span style="font-size:9pt;">11</span><span style="font-size:9pt;font-family:宋体;">日。</span><span style="font-size:9pt;"><span>  </span></span><span style="font-size:9pt;font-family:宋体;">目前主要是非纺织品的应用。</span><span style="font-size:9pt;"></span> <br /><br /><br />本文地址：<a href="http://www.陈忠源化学文库.cn/Article.asp?ID=10000073" target="_blank">http://www.陈忠源化学文库.cn/Article.asp?ID=10000073</a>   填写邮件内容   邮件签名     填写邮件签名 发信地址     填写发信人的电子邮箱 　验证码     填写验证码，单击即可刷新验证码   发送协议 ·欢迎使用本站在线文章发送系统。 ·不得使用本站在线发送邮件系统发送垃圾邮件、广告邮件。 ·如果收信人地址或其服务器出现错误，可能无法成功发送。 ·如果有什么问题，或者意见建议，请联系[网站管理员]。

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