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发 送 文 章     C.I. 还原红13 = C.I. 颜料红195 (C.I. 70320) [留言][评论][收藏] 收信地址     填写收信人的电子邮箱 邮件主题     填写邮件主题 邮件内容  <p class="MsoNormal"> <strong><span><span>           </span><u>C.I. </u></span></strong><strong><u><span style="font-family:宋体;">还原红</span><span>13 = C.I. </span></u></strong><strong><u><span style="font-family:宋体;">颜料红</span><span>195 (C.I. 70320) </span></u><span><span>         </span>CAS</span></strong><strong><span style="font-family:宋体;">号：</span><span>[4203-77-4]</span></strong> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;">CAS</span></u></strong><strong><u><span style="font-size:9.0pt;font-family:宋体;">名：</span></u></strong><strong><span style="font-size:9.0pt;"><span>  </span>[3,3’-Bianthra[1,9-cd]pyrazole]-6,6’(1H,1’H)-dione,</span></strong><span style="font-size:9.0pt;"> 1,1’-diethyl-</span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">发明者：</span></u></strong><span style="font-size:9.0pt;"><span>  </span>F. Singer and A. Holl 1914</span><span style="font-size:9.0pt;font-family:宋体;">年。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">生产工艺文献：</span></u></strong><strong><span style="font-size:9.0pt;"><span>  </span>BIOS 987, </span></strong><span style="font-size:9.0pt;">128-9.<span>  </span><strong>Indanthrene Rubine R<span>  </span></strong></span><span style="font-size:9.0pt;font-family:宋体;">英译文。详见原文。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><span style="font-size:9.0pt;"><span>                </span>FIAT 1313,II, </span></strong><span style="font-size:9.0pt;">162-3. <strong>Indanthrene Rubine R<span>  </span></strong></span><span style="font-size:9.0pt;font-family:宋体;">英译文。详见原文。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span>                </span><strong>PB 74026,</strong> 2752-4.<span>  </span><strong>Indanthrenrubin R<span>  </span></strong></span><span style="font-size:9.0pt;font-family:宋体;">德文。非工艺原件。译文如下。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span>         </span></span><strong><u><span style="font-size:9.0pt;font-family:宋体;">阴丹士林红玉</span></u></strong><strong><u><span style="font-size:9.0pt;">R </span></u></strong><strong><u><span style="font-size:9.0pt;font-family:宋体;">生产工艺规程</span></u></strong><strong><u><span style="font-size:9.0pt;"> </span></u></strong><strong><span style="font-size:9.0pt;"><span>                  </span>Mainkur<span>  </span>1938</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">年</span></strong><strong><span style="font-size:9.0pt;">11</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">月</span></strong><strong><span style="font-size:9.0pt;">14</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">日。</span></strong><strong><span style="font-size:9.0pt;"></span></strong> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">反应式：</span></u></strong><span style="font-size:9.0pt;"><span>  </span></span><span style="font-size:9.0pt;font-family:宋体;">（本人有加注）</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><img src="data:image/png;base64,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" alt="" /></span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal" style="text-indent:9.0pt;"> <span style="font-size:9.0pt;font-family:宋体;">蒽并吡唑酮</span><span style="font-size:9.0pt;"><span>                                                 </span></span><span style="font-size:9.0pt;font-family:宋体;">酸式</span><span style="font-size:9.0pt;">= </span><span style="font-size:9.0pt;font-family:宋体;">联二蒽并吡唑酮</span><span style="font-size:9.0pt;"> (C.I. 70315)</span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><img src="data:image/png;base64,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" alt="" /></span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"><span>        </span>C.I. 70315<span>                        </span></span><span style="font-size:9.0pt;font-family:宋体;">对甲苯磺酸乙酯</span><span style="font-size:9.0pt;"><span>             </span>C.I. </span><span style="font-size:9.0pt;font-family:宋体;">还原红</span><span style="font-size:9.0pt;">13 (C.I. 70320)</span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">操作步骤：</span></u></strong><strong><u><span style="font-size:9.0pt;"></span></u></strong> <br /> <p class="MsoNormal"> <u><span style="font-size:9.0pt;">1. </span></u><u><span style="font-size:9.0pt;font-family:宋体;">吡唑黄钾盐：</span></u><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal" style="text-indent:18.0pt;"> <span style="font-size:9.0pt;">147</span><span style="font-size:9.0pt;font-family:宋体;">公斤<strong>吡唑蒽酮</strong>和</span><span style="font-size:9.0pt;">292</span><span style="font-size:9.0pt;font-family:宋体;">公斤<strong>苛性钾</strong>于鼓磨中混合研磨三小时，将其加到</span><span style="font-size:9.0pt;">2000</span><span style="font-size:9.0pt;font-family:宋体;">升反应锅内，由计量槽加入</span><span style="font-size:9.0pt;">60</span><span style="font-size:9.0pt;font-family:宋体;">公斤<strong>乙醇</strong>，密闭设备，开动搅拌，反应立即开始，无需加热，约在一小时内升温到</span><span style="font-size:9.0pt;">100<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">，然后加热到</span><span style="font-size:9.0pt;">125-130<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">，保温反应</span><span style="font-size:9.0pt;">6</span><span style="font-size:9.0pt;font-family:宋体;">小时，压力约为</span><span style="font-size:9.0pt;">2.5</span><span style="font-size:9.0pt;font-family:宋体;">大气压，反应完后冷却至</span><span style="font-size:9.0pt;">110<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">，放压，在</span><span style="font-size:9.0pt;">4</span><span style="font-size:9.0pt;font-family:宋体;">小时内以细流状加入</span><span style="font-size:9.0pt;">700</span><span style="font-size:9.0pt;font-family:宋体;">升水，使物料溶解，约</span><span style="font-size:9.0pt;">8</span><span style="font-size:9.0pt;font-family:宋体;">小时后（从加水开始计算）将料液压人</span><span style="font-size:9.0pt;">5300</span><span style="font-size:9.0pt;font-family:宋体;">升铁锅内，用</span><span style="font-size:9.0pt;">60<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">热水稀释至</span><span style="font-size:9.0pt;">4000</span><span style="font-size:9.0pt;font-family:宋体;">升，在</span><span style="font-size:9.0pt;">60<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">通空气氧化</span><strong><span style="font-size:9.0pt;">12</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">小时</span></strong><span style="font-size:9.0pt;font-family:宋体;">，吡唑黄钾盐析出（<strong>取样</strong></span><strong><span style="font-size:9.0pt;">1.</span></strong><span style="font-size:9.0pt;font-family:宋体;">），压滤，滤饼不用洗涤，但需吹干，再送入水压机内用</span><span style="font-size:9.0pt;">80</span><span style="font-size:9.0pt;font-family:宋体;">大气压压干，最后在</span><span style="font-size:9.0pt;">95-100<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">减压烘干。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal" style="text-indent:18.0pt;"> <strong><span style="font-size:9.0pt;font-family:宋体;">得量：</span></strong><span style="font-size:9.0pt;font-family:宋体;">约为</span><span style="font-size:9.0pt;">170</span><span style="font-size:9.0pt;font-family:宋体;">公斤工业品。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <u><span style="font-size:9.0pt;">2. </span></u><u><span style="font-size:9.0pt;font-family:宋体;">二乙基红：</span></u><u><span style="font-size:9.0pt;"></span></u> <br /> <p class="MsoNormal" style="text-indent:18.0pt;"> <span style="font-size:9.0pt;font-family:宋体;">上述吡唑黄钾盐，于研磨锅中，加入</span><span style="font-size:9.0pt;">270</span><span style="font-size:9.0pt;font-family:宋体;">升</span><span style="font-size:9.0pt;">=292</span><span style="font-size:9.0pt;font-family:宋体;">公斤氯甲苯，研磨</span><span style="font-size:9.0pt;">18</span><span style="font-size:9.0pt;font-family:宋体;">小时，放入<strong>乙基化锅</strong>内（<strong>取样</strong></span><strong><span style="font-size:9.0pt;">2.</span></strong><span style="font-size:9.0pt;font-family:宋体;">）研磨锅用氯甲苯洗三次，每次</span><span style="font-size:9.0pt;">400</span><span style="font-size:9.0pt;font-family:宋体;">升</span><span style="font-size:9.0pt;">=432</span><span style="font-size:9.0pt;font-family:宋体;">公斤，加入</span><span style="font-size:9.0pt;">150</span><span style="font-size:9.0pt;font-family:宋体;">公斤<strong>对甲苯磺酸乙酯</strong>和</span><span style="font-size:9.0pt;">16</span><span style="font-size:9.0pt;font-family:宋体;">公斤<strong>苛性钾，</strong>在</span><span style="font-size:9.0pt;">125<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">反应</span><span style="font-size:9.0pt;">9</span><span style="font-size:9.0pt;font-family:宋体;">小时，同时蒸出带少量水的氯甲苯，冷至</span><span style="font-size:9.0pt;">110<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">，用压滤吸滤器过滤，滤饼用氯甲苯洗涤四次，每次</span><span style="font-size:9.0pt;">500</span><span style="font-size:9.0pt;font-family:宋体;">升</span><span style="font-size:9.0pt;">=541</span><span style="font-size:9.0pt;font-family:宋体;">公斤（<strong>取样</strong></span><strong><span style="font-size:9.0pt;">3.</span></strong><span style="font-size:9.0pt;font-family:宋体;">）。将氯甲苯液放入反应锅内，蒸出氯甲苯（<strong>取样</strong></span><strong><span style="font-size:9.0pt;">4.</span></strong><span style="font-size:9.0pt;font-family:宋体;">）。氯甲苯回收。略！</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <u><span style="font-size:9.0pt;">3. </span></u><u><span style="font-size:9.0pt;font-family:宋体;">士林红玉</span></u><u><span style="font-size:9.0pt;">R</span></u><u><span style="font-size:9.0pt;font-family:宋体;">：</span></u><u><span style="font-size:9.0pt;"></span></u> <br /> <p class="MsoNormal" style="text-indent:18.0pt;"> <span style="font-size:9.0pt;font-family:宋体;">将二批二乙基红加入预先加有</span><span style="font-size:9.0pt;">1480</span><span style="font-size:9.0pt;font-family:宋体;">公斤</span><strong><span style="font-size:9.0pt;">60</span></strong><sup><span style="font-size:9.0pt;">0</span></sup><span style="font-size:9.0pt;font-family:宋体;">波美<strong>硫酸</strong>的</span><span style="font-size:9.0pt;">3000</span><span style="font-size:9.0pt;font-family:宋体;">升反应锅内，于</span><span style="font-size:9.0pt;">40<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">搅拌十小时至溶解，冷至</span><span style="font-size:9.0pt;">20<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">，压人加有</span><span style="font-size:9.0pt;">6800</span><span style="font-size:9.0pt;font-family:宋体;">升水和</span><span style="font-size:9.0pt;">20</span><span style="font-size:9.0pt;font-family:宋体;">公斤<strong>保护剂</strong>的</span><span style="font-size:9.0pt;">20000</span><span style="font-size:9.0pt;font-family:宋体;">升稀释锅内，析出温度约升到</span><span style="font-size:9.0pt;">40-45<sup>0</sup>C.</span><span style="font-size:9.0pt;font-family:宋体;">，搅拌一小时，用二台压滤机压滤，吹干。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal" style="text-indent:18.0pt;"> <strong><span style="font-size:9.0pt;font-family:宋体;">得量：</span></strong><span style="font-size:9.0pt;font-family:宋体;">约</span><span style="font-size:9.0pt;"> 1100</span><span style="font-size:9.0pt;font-family:宋体;">公斤膏状物，干品含量</span><span style="font-size:9.0pt;">18-20%</span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">溶剂损耗量：</span></u></strong><span style="font-size:9.0pt;"><span>  </span></span><span style="font-size:9.0pt;font-family:宋体;">氯甲苯损耗约</span><span style="font-size:9.0pt;">4%</span><span style="font-size:9.0pt;font-family:宋体;">。</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <strong><u><span style="font-size:9.0pt;font-family:宋体;">取样分析：</span></u></strong><span style="font-size:9.0pt;"><span>  </span></span><span style="font-size:9.0pt;font-family:宋体;">略！</span><span style="font-size:9.0pt;"><span>     </span></span><strong><u><span style="font-size:9.0pt;font-family:宋体;">操作要点：</span></u></strong><span style="font-size:9.0pt;"><span>  </span></span><span style="font-size:9.0pt;font-family:宋体;">略！</span><span style="font-size:9.0pt;"><span>     </span></span><strong><u><span style="font-size:9.0pt;font-family:宋体;">生产设备：</span></u></strong><span style="font-size:9.0pt;"><span>  </span></span><span style="font-size:9.0pt;font-family:宋体;">略！</span><span style="font-size:9.0pt;"></span> <br /> <p class="MsoNormal"> <span style="font-size:9.0pt;"> </span> <br /> <p class="MsoNormal"> <strong><span style="font-size:9.0pt;font-family:宋体;">陈忠源</span></strong><strong><span style="font-size:9.0pt;"><span>   </span>2016</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">年</span></strong><strong><span style="font-size:9.0pt;">3</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">月</span></strong><strong><span style="font-size:9.0pt;">2</span></strong><strong><span style="font-size:9.0pt;font-family:宋体;">日</span></strong><strong><span style="font-size:9.0pt;"></span></strong> <br /><br /><br />本文地址：<a href="http://www.陈忠源化学文库.cn/Article.asp?ID=10000063" target="_blank">http://www.陈忠源化学文库.cn/Article.asp?ID=10000063</a>   填写邮件内容   邮件签名     填写邮件签名 发信地址     填写发信人的电子邮箱 　验证码     填写验证码，单击即可刷新验证码   发送协议 ·欢迎使用本站在线文章发送系统。 ·不得使用本站在线发送邮件系统发送垃圾邮件、广告邮件。 ·如果收信人地址或其服务器出现错误，可能无法成功发送。 ·如果有什么问题，或者意见建议，请联系[网站管理员]。

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